HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 53704383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-Chlorobenzyl cyanide | HCID 241582 | — |
| Reactant | 4-(4-Chlorobutyl)-2,6-dimethylmorpholine hydrochloride | HCID 19738024 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 53704383 | HCID 53704383 | — |
Reaction Steps
This intermediate (400 mg.) was prepared using the procedure described in Example 2a except using 1.0 g. (4.13 mmoles) of 4-(4-chlorobutyl)-2,6-dimethylmorpholine hydrochloride, 1.81 g. (0.021 mole) of sodium hydride, and 3.18 g. (0.021 mole) of 4-chlorobenzyl cyanide in 40 ml. of DMF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240925 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-810bb6e4eaed421c8dfdf8eb024a1639 |
| Source note | uspto-grants-1993_08 |