Carbon Tetrachloride → HCID 19738027, compound

HRID 2255380Notes

Reaction equation

HRID 2255380 reaction equation
[CH3:1][CH:2]1[O:7][CH:6]([CH3:8])[CH2:5][N:4]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19]O)[CH2:3]1.C1(P(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1.C(Cl)(Cl)(Cl)[Cl:41]>>[Cl:41][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][N:4]1[CH2:3][CH:2]([CH3:1])[O:7][CH:6]([CH3:8])[CH2:5]1

Participants

4

Reactant 3

HCID 5943Carbon TetrachlorideHCID 11776TriphenylphosphineHCID 19738047HCID 19738047, compound

Product 1

HCID 19738027HCID 19738027, compound

Procedure

This intermediate (5.1 g.) was prepared using the procedure described in Example 4c except using 9.35 g. (0.033 mole) of 2,6-dimethyl-4-(11-hydroxyundecyl)morpholine, 9.43 g. (0.036 mole) of triphenylphosphine, and 70 ml. of carbon tetrachloride.

Workup

  1. customThis intermediate (5.1 g.) was prepared

Sources & evidence

ORD record
ord-27053404a0234d7ca45156eaa220ff7b
Source dataset
uspto-grants-1993_08
Patent number
US05240925

Reaction notes

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