HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 19738035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Chloromethyl-1H-1,2,4-triazole | HCID 3743882 | — |
| Reactant | HCID 19738034 | HCID 19738034 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19738035 | HCID 19738035 | — |
Reaction Steps
This compound (350 mg.) was prepared using the procedure described in Example 2b except using 500 mg. (1.25 mmoles) of 2-(4-chlorophenyl)-13-(2,6-dimethyl-4-morpholinyl)tridecanonitrile, 60 mg (1.35 mmoles) of sodium hydride, 150 mg. (1.25 mmoles) of 1-(chloromethyl)-1,2,4-triazole, and 15 ml. of DMF and was isolated as an amber oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240925 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-c6ca4e0018b141a0aa0b22dcc4e2f623 |
| Source note | uspto-grants-1993_08 |