HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19738030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N-(3-chloropropyl)piperidine hydrochloride | HCID 79624 | — |
| Reactant | 2,4-Dichlorophenylacetonitrile | HCID 80566 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 19738030 | HCID 19738030 | — |
Reaction Steps
This intermediate (10 g.) was prepared using the procedure described in Example 14a except using 10.0 g. (0.054 mole) of 2,4-dichlorobenzyl cyanide, 11.0 g. (0.054 mole) of 1-(3-chloropropyl)piperidine hydrochloride, 11.0 g. (0.135 mole) of 50% aqueous sodium hydroxide, and 50 ml. of DMSO.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240925 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-d28103a3ffe14259b9ccec03afb7b366 |
| Source note | uspto-grants-1993_08 |