HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19737967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sulfur Dioxide | HCID 1119 | — |
| Reactant | hydroxylamine-O-sulfonic acid | HCID 76284 | — |
| Reactant | HCID 19874047 | HCID 19874047 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 19737967 | HCID 19737967 | — |
Reaction Steps
The product from Step A (1.84 g, 5.79 mmol) was treated sequentially with n-butyllithium (2.2 equivalents), sulfur dioxide, hydroxylamine-O-sulfonic acid and methanolic HCl in much the same was as described in Example 4 to furnish the desired product as a white solid: mp 118°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240923 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-bf7fd0f61d604d198422416f82eea0be |
| Source note | uspto-grants-1993_08 |