N-Methoxy-N-methylacetamide → HCID 57753537, compound

HRID 225557Notes

Reaction equation

HRID 225557 reaction equation
[CH:1]([N:4]([CH:17]([CH3:19])[CH3:18])[C:5]([C:7]1[CH:12]=[CH:11][C:10]([C:13]([F:16])([F:15])[F:14])=[CH:9][N:8]=1)=[O:6])([CH3:3])[CH3:2].CON(C)[C:23](=[O:25])[CH3:24]>>[CH:17]([N:4]([CH:1]([CH3:3])[CH3:2])[C:5]([C:7]1[C:12]([C:23](=[O:25])[CH3:24])=[CH:11][C:10]([C:13]([F:16])([F:14])[F:15])=[CH:9][N:8]=1)=[O:6])([CH3:19])[CH3:18]

Participants

3

Reactant 2

HCID 537505N-Methoxy-N-methylacetamideHCID 58688001HCID 58688001, compound

Product 1

HCID 57753537HCID 57753537, compound

Procedure

Prepared in analogy to Example A17(b) from 5-Trifluoromethyl-pyridine-2-carboxylic acid diisopropylamide (CAS: 765298-31-5) and N-methoxy-N-methylacetamide instead of dimethylformamide. Orange solid. MS (m/e): 317.1 ([M+H]+, 100%)

Sources & evidence

ORD record
ord-9b593471494d4edbb3aaca3a3fa8670b
Source dataset
uspto-grants-2009_07
Patent number
US07557114B2

Reaction notes

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