Timonacic → HCID 54120114, compound

HRID 2255709Notes

Reaction equation

HRID 2255709 reaction equation
[CH2:1]([N:4]([CH2:10][CH:11]=O)[C:5](=[O:9])[O:6][CH2:7][CH3:8])[CH:2]=[CH2:3].[S:13]1[CH2:17][CH:16](C(O)=O)[NH:15][CH2:14]1>C1(C)C=CC=CC=1>[N:15]12[CH2:14][S:13][CH2:17][CH:16]1[CH2:3][CH:2]1[CH:11]2[CH2:10][N:4]([C:5]([O:6][CH2:7][CH3:8])=[O:9])[CH2:1]1

Participants

4

Reactant 2

HCID 9934TimonacicHCID 11084330Ethyl allyl(2-oxoethyl)carbamate

Product 1

HCID 54120114HCID 54120114, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

17.2 g (0.1 mol) of ethyl N-allyl-N-(2-oxoethyl)-carbamate are heated under reflux overnight with 13.5 g (0.1 mol) of thiazolidine-4-carboxylic acid in 300 ml of toluene. The mixture is concentrated and the residue is distilled.

Workup

  1. concentrationThe mixture is concentrated
  2. distillationthe residue is distilled

Sources & evidence

ORD record
ord-a736efce6445414fbd99baf85e51afc0
Source dataset
uspto-grants-1993_08
Patent number
US05241076

Reaction notes

Loading…