HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 22924376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 1-Benzyloctahydropyrrolo[3,4-b]pyrrole | HCID 22562208 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 22924376 | HCID 22924376 | — |
Reaction Steps
10.8 g (46.9 mmol) of 2-benzyl-2,7-diazabicyclo[3.3.0]octane in 200 ml of ethanol are hydrogenated at 100° C. and 100 bar on 2.5 g of palladium-active carbon. The catalyst is filtered off with suction, the filtrate is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05241076 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-5883218f06ef42fe9c6578b14153a730 |
| Source note | uspto-grants-1993_08 |