HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl cyanoacetate → HCID 338194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl cyanoacetate | HCID 7764 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178503015 | HCID 178503015 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 338194 | HCID 338194 | 95.5% |
Reaction Steps
Analogously to Example 1, 27.6 g of 95.5% pure dipyrroli-dino-formamidinium methylsulphate were reacted with 11.4 g of ethyl cyanoacetate and 4.0 g of NaOH powder in 140 ml of toluene. After work-up, 95.5% of ethyl pyrrolidino-methylenecyanoacetate were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05241099 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-fde892dfad6d46d0a0d77a1a2c323d3d |
| Source note | uspto-grants-1993_08 |