Propylene Glycol → HCID 19738621, compound

HRID 2255824Notes

Reaction equation

HRID 2255824 reaction equation
Cl[C:2]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[C:9]([CH:16]=[O:17])=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[CH:7]2.[CH2:18]([OH:22])[CH:19]([OH:21])[CH3:20]>CCCCC>[OH:21][CH:19]([CH3:20])[CH2:18][O:22][C:2]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[C:9]([CH:16]=[O:17])=[C:8]2[C:3]=1[CH:4]=[CH:5][CH:6]=[CH:7]2

Participants

4

Reactant 2

HCID 1030Propylene GlycolHCID 8270310-Chloro-9-anthraldehyde

Product 1

HCID 19738621HCID 19738621, compoundYield 29.5%

Reagents, catalysts & solvents 1

HCID 8003PentaneSolvent

Procedure

Using the procedure outlined in Example 2A, 10-chloroanthracene-9-carbaldehyde (Aldrich) and 1,2-propyleneglycol (Aldrich) gave a 29.5% yield of 10-[2-(hydroxy)propoxy]anthracene-9-carbaldehyde, mp 84°-86°, (C,H), (pentane).

Sources & evidence

ORD record
ord-89d33735c64144c588a1c17a5deaffef
Source dataset
uspto-grants-1993_08
Patent number
US05241107

Reaction notes

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