HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-2-methyl-1,3-propanediol → HCID 53739728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-2-methyl-1,3-propanediol | HCID 1531 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 15050900 | HCID 15050900 | — |
| Solvent | Diethyl ether 2-propanol | HCID 22147583 | — |
| Product | HCID 53739728 | HCID 53739728 | 27.5% |
Reaction Steps
Using the procedure outlined in Example 3D except that the crude free base was treated with methanesulfonic acid, 4-bromomethylchrysene (10A) and 2-amino-2-methyl-1,3-propanediol (Aldrich) gave a 27.5% yield of 2-[(4-chrysenylmethyl)amino]-2-methyl-1,3-propanediol methanesulfonate 0.4 H2O 0.1 i-PrOH, mp 192°-193.5° (C,H,N,S), (i-PrOH/Et2O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05241107 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-3b4bd2ea9a5541bca0b9896eade2ef67 |
| Source note | uspto-grants-1993_08 |