HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dimethoxyethane → HCID 178521645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dimethoxyethane | HCID 8071 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 178521645 | HCID 178521645 | — |
Reaction Steps
A stirred solution of 10.83 g of per-0-acetyl xylitol bromide in 30 ml of dry 1,2-dimethoxyethane was added dropwise to a stirred suspension of 13.0 g of lithium aluminum hydride in 200 ml of dry 1,2-dimethoxyethane kept under nitrogen at room temperature. After this processing, 3.34 g of 1,5-anhydroxylitol was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05654280 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-07239b3b01304b769114da928a7266f7 |
| Source note | uspto-grants-1997_08 |