2-Chlorobenzoic Acid → 2-Chlorobenzoyl chloride

HRID 2255967Notes

Reaction equation

[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4](O)=[O:5].S(Cl)([Cl:13])=O>>[Cl:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([Cl:13])=[O:5]

Participants

Reactant 2

HCID 83742-Chlorobenzoic Acid

HCID 24386Thionyl Chloride

Product 1

HCID 691102-Chlorobenzoyl chloride

Procedure

As described for Reference Example 26, 3.13 g of 2-chlorobenzoic acid is reacted with 40 ml of thionyl chloride to give 3.32 of product as an off-white semi solid.

Workup

customto give 3.32 of product as an off-white semi solid

Sources & evidence

ORD record: ord-07752d24479e4f2fa9f908f99aa707f9
Source dataset: uspto-grants-1997_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05654297

Reaction notes

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