HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aminoethylpiperazine → HCID 10538710, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aminoethylpiperazine | HCID 8795 | — |
| Reactant | 4-Ethoxy-3-nitropyridine | HCID 356305 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 10538710 | HCID 10538710 | — |
Reaction Steps
A mixture of 1-(2-aminoethyl)piperazine and 4-ethoxy-3-nitropyridine in CH3CN was heated at reflux for 40 hours. The reaction mixture was cooled to ambient temperature and concentrated to give 3-nitro-4-[2-(piperazine-1-yl)ethyl]aminopyridine which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05654305 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-b47c83b98d9744ce97bd72ae13e28fcb |
| Source note | uspto-grants-1997_08 |