HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributyl(5,6-dihydro-1,4-dioxin-2-yl)stannane → 2-Benzyl-5-(5,6-dihydro-[1,4]dioxin-2-yl)-2,3-Dihydro-1H-isoindole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributyl(5,6-dihydro-1,4-dioxin-2-yl)stannane | HCID 11100832 | — |
| Reactant | 2-Benzyl-5-bromoisoindoline | HCID 53416550 | — |
| Product | 2-Benzyl-5-(5,6-dihydro-[1,4]dioxin-2-yl)-2,3-Dihydro-1H-isoindole | HCID 57753285 | — |
Reaction Steps
Prepared in analogy to Example A49(a) from 2-benzyl-5-bromo-2,3-dihydro-1H-isoindole (Example A62(a)) and tributyl-(5,6-dihydro-[1,4]dioxin-2-yl)-stannane. Light brown solid. MS (m/e): 294.4 ([M+H]+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07557114B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-6c91878463d6457ab35dc027b5d49f4c |
| Source note | uspto-grants-2009_07 |