HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 3029603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 1,8-Octanediamine | HCID 24250 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 3029603 | HCID 3029603 | — |
Reaction Steps
Combine 14.4 g (0.1 mol) of 1,8-octanediamine, 20.3 ml (0.2 mol) of benzaldehyde, 0.3 g PtO2 and 150 ml ethanol and treat the mixture with H2 at 45 lb/in2 in a shaker flask until no more gas is taken up. Remove the catalyst by filtration and remove the solvent at reduced pressure to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05654484 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-0dac1686039d46e2b5625156d6abfaec |
| Source note | uspto-grants-1997_08 |