Benzaldehyde → HCID 3029603, compound

HRID 2256641Notes

Reaction equation

HRID 2256641 reaction equation
[CH2:1]([NH2:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][NH2:9].[CH:11](=O)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>O=[Pt]=O.C(O)C>[C:12]1([CH2:11][NH:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][NH:10][CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

5

Reactant 2

HCID 240BenzaldehydeHCID 242501,8-Octanediamine

Product 1

HCID 3029603HCID 3029603, compound

Reagents, catalysts & solvents 2

HCID 345198Adams' catalystCatalystHCID 702EthanolSolvent

Procedure

Combine 14.4 g (0.1 mol) of 1,8-octanediamine, 20.3 ml (0.2 mol) of benzaldehyde, 0.3 g PtO2 and 150 ml ethanol and treat the mixture with H2 at 45 lb/in2 in a shaker flask until no more gas is taken up. Remove the catalyst by filtration and remove the solvent at reduced pressure to yield the title compound.

Workup

  1. customRemove the catalyst
  2. filtrationby filtration
  3. customremove the solvent at reduced pressure

Sources & evidence

ORD record
ord-0dac1686039d46e2b5625156d6abfaec
Source dataset
uspto-grants-1997_08
Patent number
US05654484

Reaction notes

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