Nitrogen → HCID 14585908, compound

HRID 2256642Notes

Reaction equation

HRID 2256642 reaction equation
[C:1]1([CH2:7][NH:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH:17][CH2:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH:25]([C:27]([CH3:29])=[O:28])=[CH2:26].N#N>CO>[O:28]=[C:27]([CH3:29])[CH2:25][CH2:26][N:17]([CH2:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][N:8]([CH2:26][CH2:25][C:27](=[O:28])[CH3:29])[CH2:7][C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

5

Reactant 3

HCID 947NitrogenHCID 6570Methyl vinyl ketoneHCID 3029603HCID 3029603, compound

Product 1

HCID 14585908HCID 14585908, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Dissolve the product obtained in Step A in 1400 ml of methanol and introduce 21.6 of methyl vinyl ketone on a stream of N2 gas. Stir for 16 hours to yield the title compound.

Sources & evidence

ORD record
ord-b094559b775541a19c35a1a4e6be2ccb
Source dataset
uspto-grants-1997_08
Patent number
US05654484

Reaction notes

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