HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitroimidazole → N-(4-Methylpent-3-en-1-yl)-2-nitroimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitroimidazole | HCID 10701 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Bromo-2-methyl-2-pentene | HCID 137521 | — |
| Product | N-(4-Methylpent-3-en-1-yl)-2-nitroimidazole | HCID 15186012 | — |
Reaction Steps
5-Bromo-2-methyl-2-pentene (15 g, 0.092 mol) was added to a slurry of 2-nitroimidazole (10.4 g, 0.092 mol) and potassium carbonate (12.7 g, 0.092 mol) and refluxed for 24 hrs. Acetone was removed on a rotary evaporator and the residue was purified by column chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656254 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-a2276d97f4c24016a52215907da0cf84 |
| Source note | uspto-grants-1997_08 |