HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 13686733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3a,4,7,7a-Tetrahydro-2-hydroxy-4,7-methano-1H-isoindole-1,3(2H)-dione | HCID 89529 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 13686733 | HCID 13686733 | — |
Reaction Steps
N-Hydroxy-norborn-5-ene-2,3-dicarboximide (17.92 g, 0.1 mole) is largely dissolved in 100 mL chloroform and 21 mL (0.15 moles) triethylamine, followed by adding 19 mL (0.2 moles) acetic anhydride at 0° C. with stirring. After stirring for 2 hours at room temperature, the solvent is largely removed, the residue is mixed with water and the precipitate is filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656601 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-11bac359b9ce4ad5bae21f369427da61 |
| Source note | uspto-grants-1997_08 |