HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22874412, compound → HCID 22874407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22874412 | HCID 22874412 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 22874407 | HCID 22874407 | 97% |
Reaction Steps
A solution of benzyl (2R)-2-t-butoxycarbonylmethyl-4-methylvalerate (3.40 g) in TFA (60 ml) was stirred for 1 hour under ice-bath cooling. Evaporation of TFA gave benzyl (2R)-2-carboxymethyl-4-methylvalerate (2.72 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656604 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-000c91d9473a45fa8e4a2d200d0dd861 |
| Source note | uspto-grants-1997_08 |