HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131718333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanesulfonamide | HCID 72879 | — |
| Reactant | Boc-D-phenylalanine | HCID 637610 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131718333 | HCID 131718333 | 77.3% |
Reaction Steps
Boc-D-Phe-OH (0.20 g), methanesulfonamide (79 mg) DMAP (0.11 g), WSCD.HCl (0.17 g) and DMF (4 ml) were reacted in a similar manner to that of Preparation 1-1) to give Boc-D-Phe-methanesulfonamide (0.21 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656604 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-f99f55940e6b41feaa8eeac0ecc3510e |
| Source note | uspto-grants-1997_08 |