4-Propanoylanisole → HCID 14726870, compound

HRID 2256987Notes

Reaction equation

HRID 2256987 reaction equation
[CH3:1][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][CH:6]=1)=[O:4].[C:13]([O:17][CH2:18][CH3:19])(=[O:16])[CH:14]=[O:15]>>[OH:15][CH:14]([CH:2]([CH3:1])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][CH:6]=1)=[O:4])[C:13]([O:17][CH2:18][CH3:19])=[O:16]

Participants

3

Reactant 2

HCID 671444-PropanoylanisoleHCID 70211Ethyl oxoacetate

Product 1

HCID 14726870HCID 14726870, compound

Conditions

Temperature
135 °C

Procedure

A mixture of 82 g of 4-methoxypropiophenone and 76.6 g of ethyl glyoxylate is heated at 135° C. for 15 hours.

Sources & evidence

ORD record
ord-646ff5c129104d9fbaaa0e675fd33990
Source dataset
uspto-grants-1997_08
Patent number
US05656631

Reaction notes

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