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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2257109Generated: November 3, 2026

Trifluoroacetic acid → HCID 22943378, compound

https://huagongshe.com/reaction/2257109

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 57242741HCID 57242741—
SolventTolueneHCID 1140—
SolventDichloromethaneHCID 6344—
ProductHCID 22943378HCID 22943378—

Reaction Steps

The compound of example 60 (1.00 g) is treated with 50% trifluoroacetic acid in dichloromethane (10 mL) for 1 hour at 0° C., and 3 hours at room temperature. The solution is diluted with toluene (50 mL) and the solvent is removed in vacuo to afford the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05656645
Source datasetuspto-grants-1997_08
ORD IDord-0be03d1d67594579b9e499ae0f644ffa
Source noteuspto-grants-1997_08