HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19027820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | HCID 19027884 | HCID 19027884 | — |
| Product | HCID 19027820 | HCID 19027820 | — |
Reaction Steps
5-Nitro-6-methylthiophthalazine, prepared as described by Sturrock et al., Can. J, Chem., 49, 3047 (1971) and Hirsch & Orphanos, J. Heterocyclic Chem., 2, 206 (1965), was reduced with tin (II ) chloride and HCl to yield 5-amino-6-methylthiophthalazine. This material was coupled with commercially available oleoyl chloride to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656634 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-40b44d0c557a4fbe9a1a18b387cc4041 |
| Source note | uspto-grants-1997_08 |