HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131720114, compound → HCID 131720113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131720114 | HCID 131720114 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 131720113 | HCID 131720113 | — |
Reaction Steps
A solution of 0.69 g of said compound in 12 ml of MeOH is hydrolysed at r.t. with 9.3 ml of the LiOH in MeOH-H2O solution, to give 0.4 g of 3-(pyrid-2-yl)-2-hydroxy-2-carboxypropanoic acid lithium salt, m.p. >300° C., I.R (nujol) 3400, 1640 cm-1HNMR (D2O) δ (TMS): 3.4 S, 7.2-7.35 m, 7.65-7.8 m, 6.3-8.4 m.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656656 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-ccb223464d4a4b8d947ac0a98031ec0f |
| Source note | uspto-grants-1997_08 |