HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 22922984, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Succinimide | HCID 11439 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 22922977 | HCID 22922977 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 22922984 | HCID 22922984 | — |
Reaction Steps
A mixture of methyl 3-methyl-2-(2,2-dimethylpropanoyl)benzoate, N-bromosuccinimide and benzoylperoxide in of anhydrous carbon tetrachloride is stirred at reflux for about 1.5 hours. After cooling to room temperature the formed succinimide is collected by suction and washed with cold carbon tetrachloride. The mother liquors are evaporated to dryness in vacuo and the residue is rinsed with diethyl ether and collected by suction filtration to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05658587 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-9351640a86684d0485dc7dc4ce1890a8 |
| Source note | uspto-grants-1997_08 |