HCID 87596239, compound → HCID 87596248, compound

Participants

Reaction Steps

The title compound was prepared from the compound of Example 11 in a similar manner to the compound of Example 2 as a white lyophilised powder (64%). δH NMR (d6 DMSO) 8.80 (1H, d, J 9.6 Hz), 7.98 (1H, d, J 8.2 Hz), 7.85 (2H, s), 7.14 (2H, m), 4.57 (1H, m), 3.96 (2H, t, J 8.2 Hz), 3.21 (1H, dd, J 13.6 and 3.7 Hz), 3.04 (2H, m), 2.92 (1H, dd, J 13.6 and 10.6 Hz), 1.44 (10H, br m), m/z (ES+, 70 eV) 550 (M+H)+.

Provenance & Evidence