HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 87596154, compound → HCID 87596536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 87596154 | HCID 87596154 | — |
| Reactant | HCID 87596239 | HCID 87596239 | — |
| Product | HCID 87596536 | HCID 87596536 | — |
Reaction Steps
The title compound was prepared from the compound of Example 30 in a similar manner to the compound of Example 2 as a white solid (78 mg, 61%). δH NMR (d6 DMSO) 8.82 (2H, s), 8.02 (0.88H, d) & 5.73 (0.12H, d), 8.74 (0.12H, d) & 7.19 (0.88H, s), 7.13 (0.88H, d) & 6.80 (0.12H, t), 4.56 (1H, br m), 3.74 (2H, t, J 8.1 Hz), 3.11 (4H, m), 0.82 (3H, s), 0.80 (3H, s). m/z (ES+, 70V) 508 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07557130B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-fb934af7076b4edbabb0007a94381462 |
| Source note | uspto-grants-2009_07 |