HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68843691, compound → HCID 68846184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68843691 | HCID 68843691 | — |
| Reactant | HCID 87596239 | HCID 87596239 | — |
| Product | HCID 68846184 | HCID 68846184 | — |
Reaction Steps
The title compound was prepared from the compound of Example 34 in a similar manner to the compound of Example 2 as a white solid (114.7 mg, 74.5%). δH NMR (d6 DMSO) 8.82 (2H, s), 8.03 (0.86H, d) & 5.74 (0.14H, d), 8.97 (0.15H, d) & 7.20 (2H, m), 7.15 (0.86H, d) & 6.80 (0.14H, d), 4.62 (1H, dd), 3.76 (2H, t, J 7.3 Hz), 3.21 (1H, dd), 3.13 (2H, t), 3.02 (1H, dd), 1.23-0.76 (8H, m), 1.04 (3H, s). m/z (ES+, 70V) 550 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07557130B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-a1e23e55d1a5490699544e5d4bddb666 |
| Source note | uspto-grants-2009_07 |