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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 225785Generated: November 1, 2026

HCID 68843691, compound → HCID 68846184, compound

https://huagongshe.com/reaction/225785

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68843691HCID 68843691—
ReactantHCID 87596239HCID 87596239—
ProductHCID 68846184HCID 68846184—

Reaction Steps

The title compound was prepared from the compound of Example 34 in a similar manner to the compound of Example 2 as a white solid (114.7 mg, 74.5%). δH NMR (d6 DMSO) 8.82 (2H, s), 8.03 (0.86H, d) & 5.74 (0.14H, d), 8.97 (0.15H, d) & 7.20 (2H, m), 7.15 (0.86H, d) & 6.80 (0.14H, d), 4.62 (1H, dd), 3.76 (2H, t, J 7.3 Hz), 3.21 (1H, dd), 3.13 (2H, t), 3.02 (1H, dd), 1.23-0.76 (8H, m), 1.04 (3H, s). m/z (ES+, 70V) 550 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07557130B2
Source datasetuspto-grants-2009_07
ORD IDord-a1e23e55d1a5490699544e5d4bddb666
Source noteuspto-grants-2009_07