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HRID2257996

反应详情

EQUATION

反应方程式

HRID 2257996 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)[C@@H](N)Cc1c[nH]c2ccccc12.Cl
HCID2734891

Methyl tryptophanate hydrochloride

C12H15ClN2O2

结构：Cl.NN=Cc1ccc(CC2CC(=O)N(CC(=O)O)C2=O)cc1
HCID67725476

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)[C@H](Cc1c[nH]c2ccccc12)NC(=O)CN1C(=O)CC(Cc2ccc(C=NN)cc2)C1=O
HCID67725084

未命名化合物

PROCEDURE

实验过程

403 mg of {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetic acid hydrochloride are coupled with 356.6 mg of L-tryptophan methyl ester hydrochloride by the process described above. After working up and chromatographic purification, 270 mg of {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetyl-L-tryptophan methyl ester are obtained.

WORKUP

后处理

  1. customchromatographic purification, 270 mg of {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetyl-L-tryptophan methyl ester
  2. customare obtained