huagongshe.com
HRID2257997

反应详情

EQUATION

反应方程式

HRID 2257997 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(N)CCc1ccccc1
HCID10856340

Methyl α-aminobenzenebutanoate

C11H15NO2

结构：Cl.NN=Cc1ccc(CC2CC(=O)N(CC(=O)O)C2=O)cc1
HCID67725476

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)C(CCc1ccccc1)NC(=O)CN1C(=O)CC(Cc2ccc(C=NN)cc2)C1=O
HCID131720120

未命名化合物

PROCEDURE

实验过程

403 mg of {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}acetic acid hydrochloride are coupled with 270 mg of D,L-homophenylalanine methyl ester by the process described above. After working up and chromatographic purification, 343 mg of {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}-acetyl-D,L-homophenylalanine methyl ester are obtained.

WORKUP

后处理

  1. customchromatographic purification, 343 mg of {3-[4-(aminoiminomethyl)benzyl]-2,5-dioxopyrrolidin-1-yl}-acetyl-D,L-homophenylalanine methyl ester
  2. customare obtained