HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Pyridin-4-yl)butan-1-amine → 8-chloro-N-[4-(4-pyridinyl)butyl]dibenzo[b,f][1,4]thiazepine-10(11H)-carboxamide, monohydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Pyridin-4-yl)butan-1-amine | HCID 13557532 | — |
| Reactant | 8-chlorodibenz[b,f][1,4]thiazepine-10(11H)-carbonyl chloride | HCID 22921716 | — |
| Product | 8-chloro-N-[4-(4-pyridinyl)butyl]dibenzo[b,f][1,4]thiazepine-10(11H)-carboxamide, monohydrochloride | HCID 131719085 | — |
Reaction Steps
The title compound of Example 49 is reacted with the product of Example 23 by the method described in Example 18 to produce the free base of the title product. This material is converted to the title compound by the method described in Example 16.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05661146 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-30293482348f474487eb2f0bc78a5677 |
| Source note | uspto-grants-1997_08 |