HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methoxy-2-(1-cyclohexenyl)benzo[b]thiophene → 6-Methoxy-2-cyclohexylbenzo[b]thiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methoxy-2-(1-cyclohexenyl)benzo[b]thiophene | HCID 23512903 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 6-Methoxy-2-cyclohexylbenzo[b]thiophene | HCID 10879420 | 49.6% |
Reaction Steps
5 g of 6-methoxy-2-(1-cyclohexenyl)benzo[b]thiophene was dissolved in 20 ml of ethyl acetate, 800 mg of 5% palladium-carbon was added, and hydrogenation was carried out at room temperature and at atmospheric pressure. The reaction mixture was filtered, and the filtrate was concentrated to obtain 2.5 g of 6-methoxy-2-cyclohexylbenzo[b]thiophene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05472962 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-5e1e3040b23446efa25e8ed91ab7e706 |
| Source note | uspto-grants-1995_12 |