HRID2259209

反应详情

EQUATION

反应方程式

HRID 2259209 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

5 g of 6-methoxy-2-(1-cyclohexenyl)benzo[b]thiophene was dissolved in 20 ml of ethyl acetate, 800 mg of 5% palladium-carbon was added, and hydrogenation was carried out at room temperature and at atmospheric pressure. The reaction mixture was filtered, and the filtrate was concentrated to obtain 2.5 g of 6-methoxy-2-cyclohexylbenzo[b]thiophene.

WORKUP

后处理

  1. customwas carried out at room temperature and at atmospheric pressure
  2. filtrationThe reaction mixture was filtered
  3. concentrationthe filtrate was concentrated