HRID2259209
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
5 g of 6-methoxy-2-(1-cyclohexenyl)benzo[b]thiophene was dissolved in 20 ml of ethyl acetate, 800 mg of 5% palladium-carbon was added, and hydrogenation was carried out at room temperature and at atmospheric pressure. The reaction mixture was filtered, and the filtrate was concentrated to obtain 2.5 g of 6-methoxy-2-cyclohexylbenzo[b]thiophene.
WORKUP
后处理
- customwas carried out at room temperature and at atmospheric pressure
- filtrationThe reaction mixture was filtered
- concentrationthe filtrate was concentrated