HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 6-Methoxy-2-methylbenzo[b]thiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 6-Methoxy-1-benzothiophene | HCID 13634237 | — |
| Product | 6-Methoxy-2-methylbenzo[b]thiophene | HCID 22143486 | 64.5% |
Reaction Steps
The same operations as in Preparation example 1 were carried out using 180 mg of 6-methoxybenzo[b]thiophene, and 450 mg of methyl iodide in place of cyclohexanone, and then purification was carried out by TLC (developing solvent, chloroform:n-hexane=1:19) to obtain 126 mg of 6-methoxy-2-methylbenzo[b]thiophene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05472962 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-c6041b427f3842f89710d39091a12f47 |
| Source note | uspto-grants-1995_12 |