HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68829449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 68829080 | HCID 68829080 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68829449 | HCID 68829449 | — |
Reaction Steps
The compound prepared in Example 1 (44 mg) was dissolved in dichloromethane (2 ml), and trifluoroacetic acid (1 ml) was added at 0□. The mixture was stirred for two hours while it was slowly warmed to room temperature, and then concentrated under reduced pressure to give the title compound (Iaa) in a stoichiometric amount.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07557133B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-346334bf7c244bbd9c3a4d16f7670cca |
| Source note | uspto-grants-2009_07 |