Ammonia → HCID 15342518, compound

Participants

Reaction Steps

50 ml of liquid ammonia was put in a sealed tube at -78° C. and 2.9 g of 3-[2-(5-hydroxytetrahydrofuran-2-yl)benzothiazol-6-yl]-5-methoxymethyl-2-oxazolidinone was added thereto. After sealing followed by stirring at room temperature for 3 h, ammonia was slowly evaporated. Acetone was added to the residue and the precipitated crystals were separated by filtration and dried to give 2.6 g of the titled compound.

Provenance & Evidence