Ethanol → HCID 23685597, compound

HRID 2259760Notes

Reaction equation

HRID 2259760 reaction equation
[OH-].[Na+:2].[CH3:3][C:4]([S:9][CH2:10][CH2:11][C:12]1[CH:20]=[CH:19][C:15]2[O:16][CH2:17][O:18][C:14]=2[CH:13]=1)([CH3:8])[C:5]([OH:7])=[O:6].C(O)C>O>[CH3:8][C:4]([S:9][CH2:10][CH2:11][C:12]1[CH:20]=[CH:19][C:15]2[O:16][CH2:17][O:18][C:14]=2[CH:13]=1)([CH3:3])[C:5]([O-:7])=[O:6].[Na+:2]

Participants

5

Reactant 3

HCID 702EthanolHCID 14798Sodium HydroxideHCID 19001629HCID 19001629, compound

Product 1

HCID 23685597HCID 23685597, compoundYield 92.4%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 0.90 g of sodium hydroxide in 9.0 ml of water was added to 6 g of 2-methyl-2-[{2-(1,3-benzodioxol-5-yl)ethyl}thio]propionic acid to obtain a solution. 100 ml of ethanol was added to the solution and the solvent was distilled off. The residue was washed with ether. After filtration, the product was dried under reduced pressure to obtain 6 g of the intended compound in the form of a white powder.

Workup

  1. customto obtain a solution
  2. distillationthe solvent was distilled off
  3. washThe residue was washed with ether
  4. filtrationAfter filtration
  5. customthe product was dried under reduced pressure

Sources & evidence

ORD record
ord-cb1d5be49b194d59a7521d76e50d38d9
Source dataset
uspto-grants-1995_12
Patent number
US05475024

Reaction notes

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