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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2259760Generated: November 1, 2026

Ethanol → HCID 23685597, compound

https://huagongshe.com/reaction/2259760

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 19001629HCID 19001629—
SolventWaterHCID 962—
ProductHCID 23685597HCID 2368559792.4%

Reaction Steps

A solution of 0.90 g of sodium hydroxide in 9.0 ml of water was added to 6 g of 2-methyl-2-[{2-(1,3-benzodioxol-5-yl)ethyl}thio]propionic acid to obtain a solution. 100 ml of ethanol was added to the solution and the solvent was distilled off. The residue was washed with ether. After filtration, the product was dried under reduced pressure to obtain 6 g of the intended compound in the form of a white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05475024
Source datasetuspto-grants-1995_12
ORD IDord-cb1d5be49b194d59a7521d76e50d38d9
Source noteuspto-grants-1995_12