Sodium Hydroxide → HCID 23694535, compound

HRID 2259785Notes

Reaction equation

HRID 2259785 reaction equation
[OH-].[Na+:2].[O:3]1[C:7]2[CH:8]=[CH:9][C:10]([CH:12]([S:16][CH2:17][C:18]([OH:20])=[O:19])[CH:13]([CH3:15])[CH3:14])=[CH:11][C:6]=2[O:5][CH2:4]1>C(O)C>[O:3]1[C:7]2[CH:8]=[CH:9][C:10]([CH:12]([S:16][CH2:17][C:18]([O-:20])=[O:19])[CH:13]([CH3:15])[CH3:14])=[CH:11][C:6]=2[O:5][CH2:4]1.[Na+:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 14514923HCID 14514923, compound

Product 1

HCID 23694535HCID 23694535, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

3.99 ml of a 2N aqueous solution of sodium hydroxide was added to 2.14 g of [{1-(1,3-benzodioxol-5-yl)-2-methyl-1-propyl}thio]acetic acid to obtain a solution, followed by the addition of ethanol. The mixture was distilled to remove the solvent. Ether was added to the obtained residue to generate a precipitate. This precipitate was separated by filtration and dried to obtain 2.2 g of the title compound as a white powder.

Workup

  1. customto obtain a solution
  2. distillationThe mixture was distilled
  3. customto remove the solvent
  4. additionEther was added to the obtained residue
  5. customThis precipitate was separated by filtration
  6. customdried

Sources & evidence

ORD record
ord-5a7ad7771adb411d84c70e3ec27fe511
Source dataset
uspto-grants-1995_12
Patent number
US05475024

Reaction notes

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