HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23694535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14514923 | HCID 14514923 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23694535 | HCID 23694535 | — |
Reaction Steps
3.99 ml of a 2N aqueous solution of sodium hydroxide was added to 2.14 g of [{1-(1,3-benzodioxol-5-yl)-2-methyl-1-propyl}thio]acetic acid to obtain a solution, followed by the addition of ethanol. The mixture was distilled to remove the solvent. Ether was added to the obtained residue to generate a precipitate. This precipitate was separated by filtration and dried to obtain 2.2 g of the title compound as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05475024 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-5a7ad7771adb411d84c70e3ec27fe511 |
| Source note | uspto-grants-1995_12 |