Diethylamine → HCID 19001636, compound

HRID 2259792Notes

Reaction equation

[CH2:1]([C:3]1[C:4]([CH2:12][CH2:13][S:14][CH2:15][C:16]([OH:18])=O)=[CH:5][C:6]2[O:10][CH2:9][O:8][C:7]=2[CH:11]=1)[CH3:2].[CH2:19]([NH:21][CH2:22][CH3:23])[CH3:20]>>[CH2:19]([N:21]([CH2:22][CH3:23])[C:16](=[O:18])[CH2:15][S:14][CH2:13][CH2:12][C:4]1[C:3]([CH2:1][CH3:2])=[CH:11][C:7]2[O:8][CH2:9][O:10][C:6]=2[CH:5]=1)[CH3:20]

Participants

Reactant 2

HCID 8021Diethylamine

HCID 22367133HCID 22367133, compound

Product 1

HCID 19001636HCID 19001636, compoundYield 87.1%

Procedure

2.1 g of the title compound was prepared from 2.0 g of [{2-(6-ethyl-1,3-benzodioxol-5-yl)ethyl}thio]-acetic acid by using 2.7 g of diethylamine as a pale yellow oil according to the same procedure as that described in Example 32.

Sources & evidence

ORD record: ord-9ffa9264b5524d969b9d7a330cac8381
Source dataset: uspto-grants-1995_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05475024

Reaction notes

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