HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 19002376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19002335 | HCID 19002335 | — |
| Product | HCID 19002376 | HCID 19002376 | 100% |
Reaction Steps
A mixture of 2-(3,4-dimethoxyphenyl)-6-phenylnicotinic acid (compound no. 303; 1.8 g; 0.0054 mole) and thionyl chloride (20 ml) is heated to boiling point under reflux for 1 h. The medium is concentrated under reduced pressure. A yellow syrup (1.9 g; yield=100%) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05475132 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-151025e7a4f542dbbee2a6f4eb05bcfa |
| Source note | uspto-grants-1995_12 |