HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Pyrazol-3-amine, 5-methyl- → HCID 178458053, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Pyrazol-3-amine, 5-methyl- | HCID 93146 | — |
| Reactant | Ethyl propanecarboximidate hydrochloride | HCID 13000588 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178458053 | HCID 178458053 | — |
Reaction Steps
A 13.8 g portion of 3-amino-5-methyl-1H-pyrazole was dissolved in 52 ml of acetonitrile, and 22.0 g of ethyl propionimidate hydrochloride was added to the above solution with cooling on an ice bath. The resulting mixture was stirred for 1 hour at the same temperature and then overnight at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05475114 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-a04b8a2956f34528bf2a98b8cd87546e |
| Source note | uspto-grants-1995_12 |