反应详情

Tetradecylamine (28.80 g, 0.13 mole) was heated to 85° C. Glycidol (10.00 g, 0.13 mole) was added dropwise. The reaction solution was heated under nitrogen for 3 hours and then was stirred overnight at room temperature. A white solid was obtained (crude yield=38.45 g). The solid was recrystalized from hot hexane (yield=12.2 g).

1. temperatureThe reaction solution was heated under nitrogen for 3 hours
2. customA white solid was obtained (crude yield=38.45 g)
3. customThe solid was recrystalized from hot hexane (yield=12.2 g)