HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl Palmitate → N-(2,3-dihydroxypropyl)-N-hexadecylhexadecanamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl Palmitate | HCID 8181 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | 3-(Hexadecylamino)propane-1,2-diol | HCID 111007 | — |
| Produkt | N-(2,3-dihydroxypropyl)-N-hexadecylhexadecanamide | HCID 15825474 | — |
Reaktionsschritte
N-(2,3-dihydroxypropyl)-N-hexadecylamine (0.40 g, 0.0013 mole) and potassium hydroxide (0.01 g, 0.18 mmole) were heated to 85° C. under vacuum. Methyl palmitate (0.343 g, 0.0013 mole) was heated to melt and added dropwise to the reaction. The reaction was heated under vacuum for 6 hours. A waxy off-white solid was obtained. The waxy solid was recrystalized from hot hexane (yield=0.4 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05476671 |
| Quelldatensatz | uspto-grants-1995_12 |
| ORD ID | ord-f73249bdb3a74b9a820d288babe2b712 |
| Quellennotiz | uspto-grants-1995_12 |