HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4S,5R)-3-(tert-Butoxycarbonyl)-2,2-dimethyl-4-phenyl-1,3-oxazolidine-5-carboxylic acid → HCID 54422886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4S,5R)-3-(tert-Butoxycarbonyl)-2,2-dimethyl-4-phenyl-1,3-oxazolidine-5-carboxylic acid | HCID 10969286 | — |
| Reactant | HCID 54436966 | HCID 54436966 | — |
| Product | HCID 54422886 | HCID 54422886 | 79.8% |
Reaction Steps
(4S,5R)-3-tert-Butoxycarbonyl-2,2-diethyl-4-phenyl-5-oxazolidinecarboxylic acid may be obtained under the conditions described in Example 6 for the preparation of (4S,5R)-3-tert-butoxycarbonyl-2,2-dimethyl-4-phenyl-5-oxazolidinecarboxylic acid. Thus, starting with 2.3 g of ethyl (4S,5R)-3-tert-butoxycarbonyl-2,2-diethyl-4-phenyl-5-oxazolidinecarboxylate, 1.7 g of (4S,5R)-3-tert-butoxycarbonyl-2,2-diethyl-4-phenyl-5-oxazolidinecarboxylic acid is obtained in the form of white crystals, melting point 185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05476954 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-45d52ba0e02a4a159994600b5513d0eb |
| Source note | uspto-grants-1995_12 |