HRID2260441

反应详情

EQUATION

反应方程式

HRID 2260441 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The title compound was prepared by the method described in Example 83, except that the title product of Example 90, Compound B, was substituted for the title product of Example 82, Compound B. The structure was supported by NMR, Ir, optical rotation (CHCl3, 25° C.; 589 nm -10.5°±2.69°; 365 nm -63.4°±18.1°), chiral HPLC (chiralpak-AD) major 98.84%, minor 0.68% (product of Example 90, Compound A) and elemental analysis.

WORKUP

后处理

  1. customThe title compound was prepared by the method