HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22857993, compound → HCID 22858006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22857993 | HCID 22857993 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 22858006 | HCID 22858006 | — |
Reaction Steps
The title compound was prepared by the method described in Example 83, except that the title product of Example 90, Compound B, was substituted for the title product of Example 82, Compound B. The structure was supported by NMR, Ir, optical rotation (CHCl3, 25° C.; 589 nm -10.5°±2.69°; 365 nm -63.4°±18.1°), chiral HPLC (chiralpak-AD) major 98.84%, minor 0.68% (product of Example 90, Compound A) and elemental analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05476944 |
| Source dataset | uspto-grants-1995_12 |
| ORD ID | ord-b5331ff9086649188a9c7814ca82c8d7 |
| Source note | uspto-grants-1995_12 |