Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2260441Generated: October 30, 2026

HCID 22857993, compound → HCID 22858006, compound

https://huagongshe.com/reaction/2260441

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 22857993HCID 22857993—
SolventChloroformHCID 6212—
ProductHCID 22858006HCID 22858006—

Reaction Steps

The title compound was prepared by the method described in Example 83, except that the title product of Example 90, Compound B, was substituted for the title product of Example 82, Compound B. The structure was supported by NMR, Ir, optical rotation (CHCl3, 25° C.; 589 nm -10.5°±2.69°; 365 nm -63.4°±18.1°), chiral HPLC (chiralpak-AD) major 98.84%, minor 0.68% (product of Example 90, Compound A) and elemental analysis.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05476944
Source datasetuspto-grants-1995_12
ORD IDord-b5331ff9086649188a9c7814ca82c8d7
Source noteuspto-grants-1995_12